Table 1. Summary of diffraction data statistics for EF1-δ(∊S65D).
The numbers in parentheses refer to the statistics for the outer-resolution shell (3.25–3.15 Å).
| Crystallization condition | 9%(w/v) PEG 8000, 0.1 M MOPS pH 7.0, 100 mM MgSO4, 4.0%(v/v) 1-propanol |
| Beamline | NSLS X29 |
| Wavelength (Å) | 1.075 |
| Space group | C2 |
| Reflections (total/unique) | 4371954/262052 |
| Unit cell | a = 433.3, b = 181.5, c = 224.2 Å, α = 90.0, β = 108.4, γ = 90.0° |
| Resolution (Å) | 60–3.15 |
| Completeness (%) | 91.4 (64.3) |
| Redundancy | 2.6 (2.1) |
| R sym † (%) | 13.9 (76.5) |
| 〈I〉/〈σ(I)〉 | 12.4 (2.3) |
†
R
sym = 
where Ii(hkl) is the ith intensity measurement of reflection hkl, including symmetry-related reflections, and 〈I(hkl)〉 is its average.