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. Author manuscript; available in PMC: 2013 Nov 16.
Published in final edited form as: J Chromatogr A. 2012 Sep 25;1264:22–30. doi: 10.1016/j.chroma.2012.09.052

Figure 13.

Figure 13

Fuse-core column stability

Column: 2.1 × 100 mm; Particles: 2.7 μm 400 Å - C8; Mobile phase - A: water/aqueous 0.1% trifluoroacetic acid; B: 70% acetonitrile/ 30% aqueous 0.1% trifluoroacetic acid; Gradient: 9 to 55% B in 10 min; Flow rate: 0.5 mL/min; Temperature: 60 °C; Injection: 1 μL; Instrument: Shimadzu Prominence; Detection: 220 nm

Peak widths measured at half-height for selected compounds (min). Peak identities as stated in Figure 6.