Table 2.

Proton NMR spectroscopy of T-2 toxin 3-glucoside (Fig. 6)

Positiona	1H shift(s) (ppm)	Mult, splitting (Hz)
1
2	3.83	d, 4.7
3	4.34	dd, 3.2, 4.7
4	5.85	d, 3.2
5
6
7ab	2.38, 2.00	dd, 15.1, 5.8; d, 15.1
8	5.34	d, 5.6
9
10	5.78	d, 5.9
11	4.46	d, 5.9
12
13ab	3.05, 2.88	d, 3.8; d, 3.8
14	0.76	S
15ab	4.38, 4.13	d, 12.4; d, 12.4
16	1.75	S
17
18ab	2.16, 2.16	M
19	2.07	M
20	0.98	d, 6.6
21	0.97	d, 6.6
22
23*	2.10	S
24
25*	2.05	S
26	4.98	d, 3.8
27	3.44	dd, 9.8, 3.8
28	3.72	t, 9.8
29	3.37	t, 9.5
30	3.59	ddd, 9.9, 4.8, 2.4
31ab	3.78, 3.70	dd, 11.9, 2.4; dd, 11.9, 4.9

^a* indicates that shifts for positions 23 and 25 may be reversed.