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. Author manuscript; available in PMC: 2013 Oct 17.
Published in final edited form as: J Am Chem Soc. 2012 Oct 3;134(41):17262–17273. doi: 10.1021/ja307497h

Scheme 13.

Scheme 13

A. Deprotection of the syn,syn-Dimer 91 (in the Absence of TBHP). B. Deprotection of the syn, syn-Dimer 91 (in the Presence of TBHP). C. Selected 1H and NOE NMR Data for the Mono Mesityl-protected Aglycon 95.