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. 2012 Oct 13;68(Pt 11):o3117. doi: 10.1107/S1600536812041906
Bruker SMART CCD diffractometer 2301 independent reflections
Radiation source: fine-focus sealed tube 1659 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.040
ω scans θmax = 25.0°, θmin = 2.5°
Absorption correction: multi-scan (SADABS; Bruker, 2002) h = −9→9
Tmin = 0.959, Tmax = 0.986 k = −7→7
3523 measured reflections l = −16→12