| Bruker SMART 1K CCD area-detector diffractometer | 3688 independent reflections |
| Radiation source: fine-focus sealed tube | 1992 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.027 |
| thin–slice ω scans | θmax = 25.1°, θmin = 2.1° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2004) | h = −9→7 |
| Tmin = 0.857, Tmax = 1.000 | k = −13→12 |
| 5308 measured reflections | l = −15→16 |
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