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. 2012 Oct 27;68(Pt 11):o3231–o3232. doi: 10.1107/S1600536812044030
Oxford Diffraction Xcalibur (Eos, Gemini) diffractometer 5265 independent reflections
Radiation source: Enhance (Cu) X-ray Source 4303 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.046
Detector resolution: 16.0416 pixels mm-1 θmax = 72.8°, θmin = 4.9°
ω scans h = −14→10
Absorption correction: multi-scan (CrysAlis PRO and CrysAlis RED; Oxford Diffraction, 2010) k = −20→21
Tmin = 0.726, Tmax = 1.000 l = −32→31
34626 measured reflections