| Oxford Diffraction Xcalibur (Eos, Gemini) diffractometer | 5265 independent reflections |
| Radiation source: Enhance (Cu) X-ray Source | 4303 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.046 |
| Detector resolution: 16.0416 pixels mm-1 | θmax = 72.8°, θmin = 4.9° |
| ω scans | h = −14→10 |
| Absorption correction: multi-scan (CrysAlis PRO and CrysAlis RED; Oxford Diffraction, 2010) | k = −20→21 |
| Tmin = 0.726, Tmax = 1.000 | l = −32→31 |
| 34626 measured reflections |