| Bruker SMART CCD area-detector diffractometer | 3824 independent reflections |
| Radiation source: fine-focus sealed tube | 1534 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.070 |
| phi and ω scans | θmax = 25.4°, θmin = 1.9° |
| Absorption correction: multi-scan (SADABS; Bruker, 2001) | h = −12→12 |
| Tmin = 0.956, Tmax = 0.971 | k = 0→11 |
| 12540 measured reflections | l = 0→16 |
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