. Author manuscript; available in PMC: 2012 Dec 17.

Published in final edited form as: Bioorg Med Chem. 2011 Jun 25;19(22):6628–6632. doi: 10.1016/j.bmc.2011.06.050

Table 2.

Selected ¹H-NMR and DEPT 135° data for 1 and its N-alkylated-KF analogs (2,4) in DMSO-d₆.

Compound	HRESIMS [M+H]⁺	¹H-NMR			¹³C-NMR
		L-Ornithine		Derivative (R) residue	L-Ornithine		Derivative (R) Residue
		NHR	C H₂(δ)	Derivative (R) residue	CH₂(δ)	NHCH₂R	Derivative (R) Residue
1	1477.9408	7.62 (m, 2H, NH₂)	2.74 (m)	7.19–7.28 (m, 5H, Ph)	38.7	-	126.8 (Ph), 128.5 (2C, Ph), 129.5 (Ph), 130.1 (Ph)
2	1599.9945	7.63 (m)	2.94 (m)	6.75–7.28 (m, 8H, Ph)	38.7	47.6	14.6 (CH₃), 114.7 (Ph), 115.0 (Ph), 126.9 (Ph), 127.5 (Ph), 128.6 (Ph), 129.7 (Ph), 130.2 (Ph), 131.6 (Ph)
4	1653.0366	7.63 (m)	2.84 (bs)	3.12 (m, 4H), 3.73 (m, 4H), 6.98–7.28 (m, 9 H, Ph)	38.4	47.6	48.5 (2×CH₂, Mor), 66.4 (2×CH₂, Mor), 115.2 (2C, Ph), 126.9 (Ph), 128.6 (2C, Ph), 129.7 (Ph), 130.3 (Ph), 131.3 (2C, Ph)

Abbreviations: Ph=phenyl, Mor=morpholine