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. Author manuscript; available in PMC: 2013 Dec 3.
Published in final edited form as: Inorg Chem. 2012 Nov 9;51(23):12660–12668. doi: 10.1021/ic301204b

Scheme 3.

Scheme 3

Synthesis of HB(RBz)3NiNO complexes 15 and 16. Reagents and conditions: (i) 0.33 HBBr2:NMe3, C6H5Cl, reflux; (ii) 1. Ag2O, MeCN or CH2Cl2, Δ; 2. Ni(NO)I(THF)2 or Ni(NO)Br(PPh3)2, THF.