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A comparison of the effect of the decoupling on the resolution of 13C INEPT spectra. High resolution is seen even at low-power WALTZ-16 [53,54] decoupling, indicating the mobile nature of the residues contributing to the INEPT spectra. Even higher resolution is observed at moderate- and high-power TPPM decoupling. All experiments were obtained on a 600-MHz Bruker spectrometer with 10 kHz MAS. The acquisition and spectral processing parameters are given in the caption to Fig. 1.
