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Selected ion monitoring (SIM) chromatogram showing putative peak (15.7 min), and mass spectrum and expected fragmentation (inset), of meMMPB in Lemieux oxidation reactions sampled by SPME (a), as well as linearity of response for peak area versus microcystin (MC-LR) concentration for SPME fibres (▲/……: PDMS-DVB, ■/ —: DVB-CAR-PDMS) evaluated in the study.
