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. Author manuscript; available in PMC: 2013 Nov 27.
Published in final edited form as: Biochemistry. 2012 Nov 13;51(47):9581–9591. doi: 10.1021/bi301132k

Table 1.

Crystallographic Data Collection and Refinement Statistics.

GCN4p1 dimer GCN4p1 trimer
space group unit cell C2 C2
   a, b, c (Å) 83.4, 30.5, 27.8 61.2, 34.4, 78.1
   α, β, γ (°) 90, 104.5, 90 90, 139.7, 90
data collection
   resolution (Å) 40.4–2.0 (2.07–2.00) 50.5–2.2 (2.28–2.20)
   Rmerge (%) 5.8 (25.3) 9.4 (22.1)
   I / σ(I) 15.5 (2.2) 9.7 (3.2)
   completeness (%) 99.8 (100.0) 99.5 (100.0)
   redundancy 3.8 (2.4) 2.7 (2.8)
refinement
   resolution (Å) 40.4–2.00 50.54–2.20
   no. reflections 4432 5198
   Rwork / Rfree (%) 23.5 / 26.5 22.6 / 28.7
   no. atoms 567 903
   avg. B factor (Å2) 23.9 24.7
rmsd
   bond lengths (Å) 0.016 0.010
   bond angles (°) 1.8 1.4