Table 1.
Data Collection and Refinement Statistics
| Data Collection and Crystal Parametersa | |
| Space group | P21 |
| Cell dimensions | |
| a, b, c (Å) | 68.9, 68.1, 97.3 |
| α, β, γ (°) | 90, 107.7, 90 |
| Wavelength (Å) | 1.0332 |
| Resolution (Å) | 50–2.24 (2.28–2.24)b |
| Rmerge (%)c | 6.5 (30.5) |
| I/σI | 17.0 (2.7) |
| Multiplicity | 3.5 (2.5) |
| Refinement | |
| Resolution (Å) | 38.8–2.24 (2.30–2.24) |
| Rwork/Rfree (%)d | 21.0/25.5 (31.1/42.3) |
| Rmsd bond lengths (Å) | 0.002 |
| Rmsd bond angles (°) | 0.579 |
a
PDB ID= 3RKP
b
Values for the highest resolution shell are shown in parentheses.
c
Rmerge= Σ|Ihkl - <Ihkl>|/ ΣIhkl, where I is the observed intensity for reflection hkl, and <I> is the mean intensity.
d
Rwork= Σ||Fo(hkl)|-|Fc(hkl)||/Σ|Fo(hkl)|; Rfree is calculated in the same way with 5% of reflections excluded from refinement.