Table 1.
Peak | Rt | Ion (−) | *Main fragments | Identification |
---|---|---|---|---|
1 | 3.58 | 631 | 479, 316, 287, 169 | Myricetin-hexosyl-gallate |
2 | 3.89 | 479 | 316, 287, 271 | Myricetin-hexoside |
3 | 3.93 | 463 | 300, 271, 255 | Quercetin-hexoside |
4 | 4.05 | 615 | 463, 300, 271, 169 | Quercetin-hexosyl-gallate |
5 | 4.20 | 615 | 463, 300, 271, 169 | Quercetin-hexosyl-gallate |
6 | 4.31 | 449 | 316, 287, 271 | Myricetin-arabinoside |
7 | 4.40 | 463 | 316, 287, 271 | Myricetin-rhamnoside |
8 | 4.55 | 599 | 447, 300, 285, 169, 124 | Quercetin-rhamnosyl-gallate |
9 | 4.70 | 653 | 501, 463, 317, 169, 124 | n.i. |
10 | 4.91 | 539 | 169, 151, 123 | n.i. |
11 | 5.05 | 433 | 301, 271, 255 | Quercetin-arabinoside |
12 | 5.28 | 447 | 301, 271, 255 | Quercetin-rhamnoside |
13 | 6.11 | 609 | 463, 300, 271 | Quercetin-rhamnosyl-hexoside |
*Negative fragment-ions.
n.i.: not identified.