Table 1. Data-collection and refinement statistics.
Values in parentheses are for the outermost resolution shell.
| Space group | C2221 |
| Unit-cell parameters (Å, °) | a = 68.03, b = 149.60, c = 74.23, α = β = γ = 90 |
| Matthews coefficient (Å3 Da−1) | 2.73 |
| Solvent content (%) | 55 |
| No. of molecules in the asymmetric unit | 1 |
| Wavelength (Å) | 1.005 |
| Light source | SSRF BL17U, U25 |
| Detector | MX225 |
| Temperature (K) | 100 |
| Resolution range (Å) | 50–2.27 |
| No. of observed reflections | 128164 |
| No. of unique reflections | 17797 |
| Completeness (%) | 99.3 (99.0) |
| 〈I/σ(I)〉 | 13.9 (1.82) |
| Multiplicity | 7.2 (7.4) |
| R merge † | 0.119 (0.446) |
R
merge =
, where Ii(hkl) is the intensity of an individual measurement of the reflection and 〈I(hkl)〉 is the mean intensity of the reflection.