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. Author manuscript; available in PMC: 2014 Jan 25.
Published in final edited form as: Carbohydr Res. 2012 Nov 21;366:33–37. doi: 10.1016/j.carres.2012.11.004

Table 3.

NMR data for non-Rha4N components of Brucella polysaccharides and OS3.

Unit H/C 1 H/C 2 H/C 3 H/C 4 H/C 5 H/C 6
PS
Glc E 4.54–4.62 3.31 3.63 3.55 3.54 3.64; 3.84
102.4 74.0 75.3 80.5 75.6 61.4
QuiNAc F 4.62 3.80 3.65 3.35 3.53 1.31
102.4 55.7 80.6 77.2 72.8 17.7
Man G 5.25 4.18 3.88 3.81 3.61 3.83; 3.83
101.9 71.2 79.4 66.7 74.6 61.7
Man H 5.11 4.28 4.02 3.77 3.82 3.77; 3.89
103.6 70.8 78.8 67.6 74.6 62.0
Man M 5.25 4.12 4.03 3.70 3.79 3.78; 3.92
101.9 79.6 71.3 68.1 74.5 62.0
OS3
QuiNAc F 4.61 3.80 3.66 3.34 3.50 1.31
102.6 55.6 80.7 77.1 72.7 17.7
Man G 5.25 4.17 3.88 3.81 3.60 3.83; 3.83
102.1 71.1 79.2 66.7 74.6 61.8
Man H 5.11 4.07 3.88 3.65 3.77 3.76; 3.90
103.4 71.2 71.5 68.0 74.5 62.3
Ery-ol 3.72 3.70 3.78 3.52; 3.71
62.0 82.9 71.5 63.5