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. 2013 Jan 10;8(1):e50504. doi: 10.1371/journal.pone.0050504

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© 2013 Mithu et al

This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are properly credited.

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2D ¹³C-¹³C spectra of A recorded at = 16.43 T and = 30 kHz. PARIS-xy (m = 1)(N = 1/2) recoupling scheme was employed during a 90 ms long mixing-time period using RF amplitudes of (a, b, c) 16 and (d, e, f) 30 kHz. Selected regions of 2D spectrum, covering (a, d) aliphatic-carbonyl, (b, e) aliphatic-aromatic, and (c, f) aliphatic-aliphatic cross-peaks, are shown in both the cases.

Inline graphic — 2D ¹³C-¹³C spectra of A recorded at = 16.43 T and = 30 kHz. PARIS-xy (m = 1)(N = 1/2) recoupling scheme was employed during a 90 ms long mixing-time period using RF amplitudes of (a, b, c) 16 and (d, e, f) 30 kHz. Selected regions of 2D spectrum, covering (a, d) aliphatic-carbonyl, (b, e) aliphatic-aromatic, and (c, f) aliphatic-aliphatic cross-peaks, are shown in both the cases.