Table 1. Data collection strategies (from Tanley et al., 2012 ▶).
Detector distance (mm) | Swing () | Sweep () | Rotation/frame () | Generator filament current (mA) | |
---|---|---|---|---|---|
Rigaku R-AXIS IV | |||||
4dd0 (3txb) | 100 | 0 | 360 | 1 | 20 |
4dd2 (3txd) | 120 | 0 | 360 | 1 | 20 |
4dd3 (3txe) | 120 | 0 | 272 | 1 | 20 |
4dd9 (3txi) | 120 | 0 | 361 | 1 | 20 |
4dda (3txj) | 135 | 0 | 181 | 1 | 20 |
4ddb (3txk) | 200 | 0 | 360 | 1 | 20 |
Bruker PLATINUM135 | |||||
4dd1 | 60† | 20 | 307.0 | 0.5 | 60 |
4dd4 (3txf) | 50† | 15.5 | 202.0 | 0.5 | 60 |
8.0 | 38.0 | ||||
12.0 | 35.0 | ||||
22.0 | 52.0 | ||||
22.0 | 63.0 | ||||
4dd6 (3txg) | 60† | 20 | 360.0 | 0.5 | 60 |
20 | 360.0 | ||||
4dd7 (3txh) | 50† | 0 | 31.0 | 0.5 | 60 |
0 | 180.0 | ||||
0 | 360.5 | ||||
20 | 360.5 | ||||
4ddc | 50† | 0 | 360.0 | 0.5 | 60 |
20 | 360.0 |
Distance from face of the detector to the phosphor plane is an additional 6.6mm.