Table 3.
The effect of sample volume on the length of glycine crystals grown from 3.2 M, pH = 6 initial solution at room temperature (RT) and using MA-MAEC technique.
| Length of crystals / μm Microwave Heating |
Length of crystals / μm Room Temperature |
|||||
|---|---|---|---|---|---|---|
| Volume/ mL |
HMA | MUDA | UDET | HMA | MUDA | UDET |
| 5 | 90-322 | 93-800 | 72-553 | 68-174 | 62-389 | 63-500 |
| 10 | 92 – 558 | 97-957 | 80-512 | 48-288 | 40-358 | 51-612 |
| 20 | 110-710 | 101-1020 | 116-788 | 52-400 | 90-350 | 70-785 |
| 50 | 177-1010 | 112-1200 | 152-1020 | 119-450 | 120-354 | 81-1250 |
| 100 | 64-950 | 110-574 | N/A# | 100-510 | 112-450 | 162-1650 |