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. 2013 Jan 21;8(1):e53999. doi: 10.1371/journal.pone.0053999

Table 1. Chemical shift data (ppm) for anomeric resonances from proton NMR spectra at 600 MHz of V. cholerae binding glycosphingolipids, and co-migrating glycosphingolipids, obtained in DMSO-d6/D2O (98∶2, by volume) at 30°C.

X IX VIII VII VI V IV III II I Fraction
A Galα3 Galβ4 GlcNAcβ3 Galβ4 Glcβ1 Cer TH-II, RE-I
4.826 4.279 4.627 4.25 4.16
B GlcNAcβ3 Galβ4 GlcNAcβ3 Galβ4 Glcβ1 Cer TH-I
4.604 4.250 4.640 4.250 4.15
C Galβ4 GlcNAcβ3 Galβ4 GlcNAcβ3 Galβ4 Glcβ1 Cer TH-II
4.20 5.643 4.253 4.643 4.253 4.16
D Galα3 Galα3 Galβ4 GlcNAcβ3 Galβ4 Glcβ1 Cer RE-I
4.826 4.893 4.28 4.66 4.25 4.16
E Galβ4 GlcNAcβ3 Galβ4 GlcNAcβ3 Galβ4 Glcβ1 Cer TH-III
4.13 4.796 4.25 4.64 4.25 4.16
F Galα3 Galβ4 GlcNAcβ3 Galβ4 GlcNAcβ3 Galβ4 Glcβ1 Cer TH-III, IV
4.826 4.279 4.626 4.257 4.78 4.257 4.16
G Galβ3 (Fucα4) GlcNAcβ3 Galβ4 Glcβ1 Cer HI-I
4.293 4.767 4.727 4.260 4.207
H Galβ3 GlcNAcβ3 Galβ3 (Fucα4) GlcNAcβ3 Galβ4 Glcβ1 Cer HI-I
4.14 4.794 4.358 4.77 4.712 4.26 4.21
I Galβ3 (Fucα4) GlcNAcβ3 Galβ3 (Fucα4) GlcNAcβ3 Galβ4 Glcβ1 Cer HI-I
4.309 4.77 4.76 4.358 4.77 4.712 4.26 4.21
J Galβ4 GlcNAcβ3 Galβ4 GlcNAcβ3 Galβ4 GlcNAcβ3 Galβ4 Glcβ1 Cer TH-IV
4.209 4.651 4.255 4.651 4.255 4.651 4.255 4.16
K Galα3 Galβ4 GlcNAcβ6 (Galα3 Galβ4 GlcNAcβ3) Galβ4 GlcNAcβ3 Galβ4 Glcβ1 Cer DE-I
4.827 4.282 4.395 4.827 4.282 4.652 4.290 4.652 4.254 4.161