Table 2.
2D-NMR data (COSY) of the compound, 5-[-3-(4-chlorophenyl)-4, 5-dihydroisoxazol-5-yl methyl]-5H dibenzo [b,f]azepine
| |
H-H-COSY |
|
1H NMR |
13C NMR |
|---|---|---|---|---|
| Position | Chemical Shifts in ppm | Position | δ ppm1H | δ ppm13C |
|
H4a |
3.153/3.208 |
|
|
|
| 3.153/4.886 |
H4ax(C-4) |
3.18 |
38.15 |
|
|
H4b |
3.208/3.153 |
|
|
|
| 3.208/4.886 |
H4eq(C-4) |
3.36 |
38.15 |
|
|
H6a |
3.483/4.295 |
|
|
|
| 3.483/4.886 |
H6a(C-6) |
3.59 |
53.7 |
|
|
H6b |
4.295/3.483 |
|
|
|
| 4.295/4.886 |
H6b(C-6) |
4.31 |
53.7 |
|
|
H5 |
4.886/3.153 |
|
|
|
| 4.886/3.208 |
|
|
|
|
| 4.886/3.483 |
|
|
|
|
| 4.886/4.296 |
H5(C-5) |
4.91 |
78.7 |
|
| |
|
C-3 |
|
155.56 |
| Ar-H | 6.5-7.7 | 120-136 |