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. Author manuscript; available in PMC: 2014 Jan 15.

Published in final edited form as: Anal Chem. 2013 Jan 3;85(2):1138–1145. doi: 10.1021/ac3030448

Table 2.

Comparison of the relative abundances of disaccharides from HSBK and HSPIM after heparin lyase digestion analyzed using SEC-MS and HILIC-MS

HSBK				HSPIM
SEC-MS		HILIC-MS		SEC-MS		HILIC-MS
D0A0	22 ± 1	D0A0	25 ± 2	D0A0	9.1 ± 0.6	D0A0	11.2 ± 0.9
D2A0/ D0A6	38 ± 2	D2A0	1.6 ± 0.2	D2A0/ D0A6	25 ± 1	D2A0	2.3 ± 0.1
D2A0/ D0A6	38 ± 2	D0A6	35 ± 2	D2A0/ D0A6	25 ± 1	D0A6	22 ± 1
D2A6	0.10 ± 0.01	D2A6	0.08 ± 0.01	D2A6	1.1 ± 0.1	D2A6	1.1 ± 0.2
D0S0	13 ± 1	D0S0	17 ± 2	D0S0	9.9 ± 0.8	D0S0	13 ± 1
D2S0/ D0S6	17 ± 1	D2S0	8.3 ± 0.4	D2S0/ D0S6	27 ± 1	D2S0	10.4 ± 0.6
D2S0/ D0S6	17 ± 1	D0S6	7.8 ± 0.5	D2S0/ D0S6	27 ± 1	D0S6	16 ± 1
D2S6	4.9 ± 0.5	D2S6	3.7 ± 0.9	D2S6	25 ± 1	D2S6	22 ± 1