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. Author manuscript; available in PMC: 2014 Jan 15.
Published in final edited form as: Anal Chem. 2013 Jan 3;85(2):1138–1145. doi: 10.1021/ac3030448

Table 2.

Comparison of the relative abundances of disaccharides from HSBK and HSPIM after heparin lyase digestion analyzed using SEC-MS and HILIC-MS

HSBK HSPIM
SEC-MS HILIC-MS SEC-MS HILIC-MS
D0A0 22 ± 1 D0A0 25 ± 2 D0A0 9.1 ± 0.6 D0A0 11.2 ± 0.9
D2A0/
D0A6		 38 ± 2 D2A0 1.6 ± 0.2 D2A0/
D0A6		 25 ± 1 D2A0 2.3 ± 0.1
D0A6 35 ± 2 D0A6 22 ± 1
D2A6 0.10 ± 0.01 D2A6 0.08 ± 0.01 D2A6 1.1 ± 0.1 D2A6 1.1 ± 0.2
D0S0 13 ± 1 D0S0 17 ± 2 D0S0 9.9 ± 0.8 D0S0 13 ± 1
D2S0/
D0S6		 17 ± 1 D2S0 8.3 ± 0.4 D2S0/
D0S6		 27 ± 1 D2S0 10.4 ± 0.6
D0S6 7.8 ± 0.5 D0S6 16 ± 1
D2S6 4.9 ± 0.5 D2S6 3.7 ± 0.9 D2S6 25 ± 1 D2S6 22 ± 1