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. Author manuscript; available in PMC: 2014 Jan 9.
Published in final edited form as: J Am Chem Soc. 2012 Dec 26;135(1):82–85. doi: 10.1021/ja311061n

Figure 1.

Figure 1

1H NMR of (A) Addition of 0.5 equiv. PhBCl2 to boronate 13 in CDCl3, followed by addition of 0.5 equiv. tBuCHO. (B) The final mixture from 30 min until completion of the reaction.