Table 2.
Summary of indirect methods
Matrix | Analyte | Pre- hydrolysis extraction | Hydrolysis | Temp (°C) | Time (min) | Post hydrolysis extraction | Clean-up | Reference |
---|---|---|---|---|---|---|---|---|
Barley | DON | ACN:water | TFA | 133 | 70 | – | C18 SPE | [52] |
Corn | DON | water | TFMSA | 22 | 20 | – | – | [53] |
Wheat | DON | water | TFMSA | 40 | 40 | – | – | [53] |
Wheat | DON | ACN:water | TCA | 140 | 40 | – | MycoSep® SPE | [104] |
Corn | FBs | SDS | 2N KOH | 60 | 60 | EtOAc | None | [65] |
Corn cereal | FBs | SDS | 2M KOH | 60 | 60 | MeOH:EDTA | HLB® | [66] |
Tortilla/chips | FBs | SDS | 2M KOH | 60 | 60 | MeOH:ACN:water | HLB® | [66] |
Corn | FBs | MeOH:water | 2M KOH | RT | 10 | ACN | – | [69] |