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. 2012 Oct 10;57(1):165–186. doi: 10.1002/mnfr.201100764

Table 2.

Summary of indirect methods

Matrix Analyte Pre- hydrolysis extraction Hydrolysis Temp (°C) Time (min) Post hydrolysis extraction Clean-up Reference
Barley DON ACN:water TFA 133 70 C18 SPE [52]
Corn DON water TFMSA 22 20 [53]
Wheat DON water TFMSA 40 40 [53]
Wheat DON ACN:water TCA 140 40 MycoSep® SPE [104]
Corn FBs SDS 2N KOH 60 60 EtOAc None [65]
Corn cereal FBs SDS 2M KOH 60 60 MeOH:EDTA HLB® [66]
Tortilla/chips FBs SDS 2M KOH 60 60 MeOH:ACN:water HLB® [66]
Corn FBs MeOH:water 2M KOH RT 10 ACN [69]