Table 5.

Comparison of full method performance for direct LC-MS/MS methods

Toxin	Other analytes	Matrix	LOD (μg/kg)	LOQ (μg/kg)	Recovery (%)	Repeatability (RSDr,%)	Reference
D3G	DON	Wheat	1	0.5	70	8	[42]
D3G	DON	Wheat	4	10	71	10	[43]
D3G	DON	Maize	4	10	130	10	[43]
D3G	7	Brewery malts	0.5	5	34–50	<10	[45]
D3G	7	Malts	N/A	1	85	5	[46]
D3G	7	Beers	1	2.5	81	6	[46]
D3G	38	Maize	4		66	5–17	[100]
D3G	9	Cereal foods	50–100	100–250	50–90	6–11	[101]
D3G	12	Maize	8	16	85	18
		Wheat	8	16	90	8
		Oats	7	14	93	12	[47]
		Cornflakes	12	24	103	5
		Bread	13	26	97	8
Z14G	ZEN	Maize	-	10	67–69	-	[64]
Z14G	38	Maize	2		100	5–22	[100]
Z14S	38	Maize	0.1		79	3–8	[100]
Z14G	9	Cereal foods	4–10	10	100–108	4–15	[101]
Z14S	9	Cereal foods	0.5–1	1–10	67–103	5–9	[101]
ZELGs	9	Cereal foods	4–10	10–25	91–111	7–10	[101]
Z14G	12	Maize	7	14	85	21
		Wheat	8	16	89	24
		Oats	9	18	88	25	[47]
		Cornflakes	10	20	83	26
		Bread	10	20	83	24