Table 2.
Summary of the crystal data and structure refinement parameters for 1, 2, and 6.
| Compound | 1 | 2 | 6 |
|---|---|---|---|
| Formula | C33H27N3 | C34H29N3 | C36H31NOS |
| Formula weight | 465.58 | 479.60 | 525.69 |
| Crystal system | Triclinic | Triclinic | Triclinic |
| Space group | P-1 | P-1 | P-1 |
| a /Å | 8.3392(13) | 8.7255(12) | 9.3797(6) |
| b /Å | 10.0974(16) | 10.8750(15) | 10.4703(6) |
| c /Å | 15.684(3) | 15.855(2) | 15.9304(10) |
| α /° | 98.756(2) | 98.469(2) | 79.5150(10) |
| β /° | 101.508(2) | 101.687(2) | 78.4040(10) |
| γ /° | 97.415(2) | 110.096(2) | 67.3940(10) |
| V /Å3 | 1261.5(4) | 1344.6(3) | 1405.30(15) |
| Z | 2 | 2 | 2 |
| Dc /Mg m−3 | 1.226 | 1.185 | 1.242 |
| μ (MoKα)/mm−1 | 0.072 | 0.070 | 0.145 |
| F(000) | 492 | 508 | 556 |
| Reflections collected/ unique |
16761/6046 [R(int)=0.0645] |
14513/4732 [R(int)=0.0434] |
15012/4944 [R(int)=0.0310] |
| Reflections with I>2σ(I) | 3370 | 4732 | 4944 |
| Goodness-of-fit on F2 | 1.001 | 1.012 | 1.043 |
| R, wR (I>2σ(I)) | 0.0585, 0.1293 | 0.0399, 0.0876 | 0.0407, 0.0988 |