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. 2013 Jan 4;69(Pt 2):o150. doi: 10.1107/S1600536812051203
O1—C1 1.2418 (17) C8—C8A 1.401 (2)
O11—C12 1.367 (2) C10—C15 1.437 (2)
O11—C15 1.3804 (19) C12—C13 1.340 (3)
N9—C8A 1.3673 (19) C13—C14 1.422 (2)
N9—C9A 1.3820 (18) C14—C15 1.363 (3)
N9—H9 0.867 (18) C3—H3A 0.9900
C1—C2 1.4867 (19) C3—H3B 0.9900
C1—C9A 1.4399 (19) C4—H4A 0.9900
C2—C3 1.513 (2) C4—H4B 0.9900
C2—C10 1.351 (2) C5—H5 0.9500
C3—C4 1.536 (2) C6—H6 0.9500
C4—C4A 1.4857 (19) C8—H8 0.9500
C4A—C9A 1.3819 (19) C10—H10 0.964 (19)
C4A—C4B 1.4227 (19) C12—H12 0.9500
C4B—C5 1.411 (2) C13—H13 0.9500
C4B—C8A 1.4144 (19) C14—H14 0.9500
C5—C6 1.375 (2) C17—H17A 0.9800
C6—C7 1.411 (3) C17—H17B 0.9800
C7—C17 1.506 (3) C17—H17C 0.9800
C7—C8 1.382 (2)
C12—O11—C15 106.77 (14) C10—C15—C14 136.41 (15)
C8A—N9—C9A 107.83 (12) O11—C15—C10 114.65 (15)
C9A—N9—H9 129.7 (12) O11—C15—C14 108.81 (14)
C8A—N9—H9 122.2 (12) C2—C3—H3A 108.00
O1—C1—C9A 121.59 (12) C2—C3—H3B 108.00
O1—C1—C2 122.91 (13) C4—C3—H3A 108.00
C2—C1—C9A 115.50 (12) C4—C3—H3B 108.00
C3—C2—C10 123.32 (12) H3A—C3—H3B 107.00
C1—C2—C3 120.81 (12) C3—C4—H4A 109.00
C1—C2—C10 115.81 (12) C3—C4—H4B 109.00
C2—C3—C4 118.19 (11) C4A—C4—H4A 109.00
C3—C4—C4A 113.51 (12) C4A—C4—H4B 109.00
C4B—C4A—C9A 106.39 (12) H4A—C4—H4B 108.00
C4—C4A—C4B 130.26 (13) C4B—C5—H5 121.00
C4—C4A—C9A 123.17 (13) C6—C5—H5 121.00
C5—C4B—C8A 118.99 (13) C5—C6—H6 119.00
C4A—C4B—C5 134.20 (14) C7—C6—H6 119.00
C4A—C4B—C8A 106.80 (12) C7—C8—H8 121.00
C4B—C5—C6 118.52 (16) C8A—C8—H8 121.00
C5—C6—C7 122.07 (16) C2—C10—H10 118.6 (12)
C6—C7—C17 119.33 (15) C15—C10—H10 113.9 (11)
C6—C7—C8 120.43 (16) O11—C12—H12 125.00
C8—C7—C17 120.25 (17) C13—C12—H12 125.00
C7—C8—C8A 117.99 (16) C12—C13—H13 127.00
N9—C8A—C8 129.24 (13) C14—C13—H13 127.00
C4B—C8A—C8 121.97 (13) C13—C14—H14 126.00
N9—C8A—C4B 108.78 (12) C15—C14—H14 126.00
C1—C9A—C4A 125.39 (12) C7—C17—H17A 109.00
N9—C9A—C1 124.41 (12) C7—C17—H17B 109.00
N9—C9A—C4A 110.20 (12) C7—C17—H17C 109.00
C2—C10—C15 127.43 (13) H17A—C17—H17B 110.00
O11—C12—C13 110.73 (16) H17A—C17—H17C 109.00
C12—C13—C14 106.59 (17) H17B—C17—H17C 109.00
C13—C14—C15 107.09 (15)
C15—O11—C12—C13 −0.7 (2) C9A—C4A—C4B—C8A 0.82 (16)
C12—O11—C15—C10 176.78 (15) C4—C4A—C9A—N9 174.68 (13)
C12—O11—C15—C14 0.2 (2) C4—C4A—C9A—C1 −4.3 (2)
C9A—N9—C8A—C4B −0.07 (16) C4B—C4A—C9A—N9 −0.89 (16)
C9A—N9—C8A—C8 −178.77 (15) C4B—C4A—C9A—C1 −179.83 (13)
C8A—N9—C9A—C1 179.56 (13) C4A—C4B—C5—C6 −178.90 (16)
C8A—N9—C9A—C4A 0.61 (16) C8A—C4B—C5—C6 1.0 (2)
O1—C1—C2—C3 173.38 (13) C4A—C4B—C8A—N9 −0.47 (16)
O1—C1—C2—C10 −4.0 (2) C4A—C4B—C8A—C8 178.34 (14)
C9A—C1—C2—C3 −6.67 (19) C5—C4B—C8A—N9 179.64 (13)
C9A—C1—C2—C10 176.00 (13) C5—C4B—C8A—C8 −1.6 (2)
O1—C1—C9A—N9 0.4 (2) C4B—C5—C6—C7 0.5 (2)
O1—C1—C9A—C4A 179.22 (14) C5—C6—C7—C8 −1.5 (3)
C2—C1—C9A—N9 −179.53 (13) C5—C6—C7—C17 178.27 (17)
C2—C1—C9A—C4A −0.7 (2) C6—C7—C8—C8A 0.9 (2)
C1—C2—C3—C4 18.4 (2) C17—C7—C8—C8A −178.87 (16)
C10—C2—C3—C4 −164.48 (14) C7—C8—C8A—N9 179.15 (15)
C1—C2—C10—C15 176.62 (14) C7—C8—C8A—C4B 0.6 (2)
C3—C2—C10—C15 −0.6 (2) C2—C10—C15—O11 169.91 (15)
C2—C3—C4—C4A −21.58 (18) C2—C10—C15—C14 −14.9 (3)
C3—C4—C4A—C4B −170.30 (14) O11—C12—C13—C14 0.8 (2)
C3—C4—C4A—C9A 15.28 (19) C12—C13—C14—C15 −0.6 (2)
C4—C4A—C4B—C5 5.6 (3) C13—C14—C15—O11 0.24 (18)
C4—C4A—C4B—C8A −174.32 (14) C13—C14—C15—C10 −175.19 (18)
C9A—C4A—C4B—C5 −179.32 (16)