| Agilent Xcalibur Ruby Gemini diffractometer | 2724 independent reflections |
| Radiation source: Enhance (Cu) X-ray Source | 2382 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.021 |
| Detector resolution: 10.5081 pixels mm-1 | θmax = 75.7°, θmin = 5.7° |
| ω scans | h = −7→7 |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2012) | k = −8→9 |
| Tmin = 0.816, Tmax = 1.000 | l = −17→17 |
| 4371 measured reflections |
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