| Nonius KappaCCD diffractometer | 2805 reflections with I > 2σ(I) |
| Radiation source: Enraf Nonius FR590 | Rint = 0.050 |
| Horizonally mounted graphite crystal monochromator | θmax = 27.5°, θmin = 2.6° |
| Detector resolution: 9 pixels mm-1 | h = −10→10 |
| CCD rotation images,thick slices scans | k = −11→10 |
| 10674 measured reflections | l = −15→15 |
| 3626 independent reflections |
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