| Rigaku R-AXIS RAPID diffractometer | 3101 independent reflections |
| Radiation source: rotaing anode | 2749 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.029 |
| Detector resolution: 10.000 pixels mm-1 | θmax = 68.3°, θmin = 4.0° |
| ω scans | h = −27→27 |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | k = −12→12 |
| Tmin = 0.693, Tmax = 0.734 | l = −17→17 |
| 28911 measured reflections |
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