| O1—C15 | 1.362 (2) | C8—C7 | 1.523 (2) |
| O1—C16 | 1.3720 (19) | C8—C10 | 1.529 (2) |
| C13—C14 | 1.342 (2) | C8—H8 | 0.9800 |
| C13—C21 | 1.451 (2) | O2—C15 | 1.207 (2) |
| C13—C9 | 1.5237 (19) | C7—C6 | 1.511 (2) |
| C21—C16 | 1.3948 (19) | C7—H7 | 0.9800 |
| C21—C20 | 1.401 (2) | C6—C5 | 1.391 (2) |
| N1—C1 | 1.386 (2) | C10—C11 | 1.522 (3) |
| N1—C9 | 1.4463 (19) | C10—H10A | 0.9700 |
| N1—H1 | 0.8600 | C10—H10B | 0.9700 |
| C16—C17 | 1.382 (2) | C2—C3 | 1.373 (3) |
| C14—C15 | 1.442 (2) | C2—H2 | 0.9300 |
| C14—H14 | 0.9300 | C22—H22A | 0.9600 |
| C9—C8 | 1.536 (2) | C22—H22B | 0.9600 |
| C9—H9 | 0.9800 | C22—H22C | 0.9600 |
| C1—C2 | 1.398 (2) | C12—C11 | 1.499 (3) |
| C1—C6 | 1.398 (2) | C12—H12A | 0.9700 |
| C17—C18 | 1.377 (2) | C12—H12B | 0.9700 |
| C17—H17 | 0.9300 | C5—C4 | 1.373 (3) |
| C18—C19 | 1.397 (2) | C5—H5 | 0.9300 |
| C18—C22 | 1.502 (2) | C4—C3 | 1.372 (3) |
| C19—C20 | 1.374 (2) | C4—H4 | 0.9300 |
| C19—H19 | 0.9300 | C3—H3 | 0.9300 |
| C20—H20 | 0.9300 | C11—H11A | 0.9700 |
| O3—C12 | 1.431 (2) | C11—H11B | 0.9700 |
| O3—C7 | 1.4316 (19) | ||
| C15—O1—C16 | 121.40 (12) | O1—C15—C14 | 117.37 (14) |
| C14—C13—C21 | 118.25 (13) | O3—C7—C6 | 112.52 (14) |
| C14—C13—C9 | 121.18 (13) | O3—C7—C8 | 111.57 (14) |
| C21—C13—C9 | 120.56 (13) | C6—C7—C8 | 111.58 (12) |
| C16—C21—C20 | 116.62 (13) | O3—C7—H7 | 106.9 |
| C16—C21—C13 | 117.98 (13) | C6—C7—H7 | 106.9 |
| C20—C21—C13 | 125.39 (13) | C8—C7—H7 | 106.9 |
| C1—N1—C9 | 120.93 (12) | C5—C6—C1 | 118.48 (16) |
| C1—N1—H1 | 119.5 | C5—C6—C7 | 121.39 (15) |
| C9—N1—H1 | 119.5 | C1—C6—C7 | 120.10 (14) |
| O1—C16—C17 | 115.72 (13) | C11—C10—C8 | 110.52 (15) |
| O1—C16—C21 | 121.83 (13) | C11—C10—H10A | 109.5 |
| C17—C16—C21 | 122.45 (15) | C8—C10—H10A | 109.5 |
| C13—C14—C15 | 123.12 (14) | C11—C10—H10B | 109.5 |
| C13—C14—H14 | 118.4 | C8—C10—H10B | 109.5 |
| C15—C14—H14 | 118.4 | H10A—C10—H10B | 108.1 |
| N1—C9—C13 | 112.47 (12) | C3—C2—C1 | 120.53 (17) |
| N1—C9—C8 | 108.27 (12) | C3—C2—H2 | 119.7 |
| C13—C9—C8 | 112.04 (12) | C1—C2—H2 | 119.7 |
| N1—C9—H9 | 108.0 | C18—C22—H22A | 109.5 |
| C13—C9—H9 | 108.0 | C18—C22—H22B | 109.5 |
| C8—C9—H9 | 108.0 | H22A—C22—H22B | 109.5 |
| N1—C1—C2 | 119.91 (14) | C18—C22—H22C | 109.5 |
| N1—C1—C6 | 120.76 (14) | H22A—C22—H22C | 109.5 |
| C2—C1—C6 | 119.33 (15) | H22B—C22—H22C | 109.5 |
| C18—C17—C16 | 120.12 (14) | O3—C12—C11 | 111.81 (16) |
| C18—C17—H17 | 119.9 | O3—C12—H12A | 109.3 |
| C16—C17—H17 | 119.9 | C11—C12—H12A | 109.3 |
| C17—C18—C19 | 118.40 (14) | O3—C12—H12B | 109.3 |
| C17—C18—C22 | 120.50 (15) | C11—C12—H12B | 109.3 |
| C19—C18—C22 | 121.10 (16) | H12A—C12—H12B | 107.9 |
| C20—C19—C18 | 121.31 (15) | C4—C5—C6 | 121.58 (18) |
| C20—C19—H19 | 119.3 | C4—C5—H5 | 119.2 |
| C18—C19—H19 | 119.3 | C6—C5—H5 | 119.2 |
| C19—C20—C21 | 120.98 (14) | C3—C4—C5 | 119.68 (18) |
| C19—C20—H20 | 119.5 | C3—C4—H4 | 120.2 |
| C21—C20—H20 | 119.5 | C5—C4—H4 | 120.2 |
| C12—O3—C7 | 112.87 (13) | C4—C3—C2 | 120.39 (18) |
| C7—C8—C10 | 110.95 (13) | C4—C3—H3 | 119.8 |
| C7—C8—C9 | 109.85 (13) | C2—C3—H3 | 119.8 |
| C10—C8—C9 | 111.42 (13) | C12—C11—C10 | 110.22 (15) |
| C7—C8—H8 | 108.2 | C12—C11—H11A | 109.6 |
| C10—C8—H8 | 108.2 | C10—C11—H11A | 109.6 |
| C9—C8—H8 | 108.2 | C12—C11—H11B | 109.6 |
| O2—C15—O1 | 117.36 (14) | C10—C11—H11B | 109.6 |
| O2—C15—C14 | 125.26 (16) | H11A—C11—H11B | 108.1 |
| C14—C13—C21—C16 | −2.2 (2) | C13—C9—C8—C10 | 171.57 (13) |
| C9—C13—C21—C16 | 176.72 (13) | C16—O1—C15—O2 | 179.89 (15) |
| C14—C13—C21—C20 | 176.89 (15) | C16—O1—C15—C14 | −0.3 (2) |
| C9—C13—C21—C20 | −4.2 (2) | C13—C14—C15—O2 | 179.75 (18) |
| C15—O1—C16—C17 | 178.94 (14) | C13—C14—C15—O1 | 0.0 (2) |
| C15—O1—C16—C21 | −0.7 (2) | C12—O3—C7—C6 | −68.9 (2) |
| C20—C21—C16—O1 | −177.22 (14) | C12—O3—C7—C8 | 57.39 (19) |
| C13—C21—C16—O1 | 2.0 (2) | C10—C8—C7—O3 | −52.89 (17) |
| C20—C21—C16—C17 | 3.2 (2) | C9—C8—C7—O3 | −176.54 (12) |
| C13—C21—C16—C17 | −177.65 (14) | C10—C8—C7—C6 | 73.92 (16) |
| C21—C13—C14—C15 | 1.3 (2) | C9—C8—C7—C6 | −49.72 (16) |
| C9—C13—C14—C15 | −177.63 (14) | N1—C1—C6—C5 | 178.45 (15) |
| C1—N1—C9—C13 | 81.22 (17) | C2—C1—C6—C5 | −0.5 (2) |
| C1—N1—C9—C8 | −43.13 (18) | N1—C1—C6—C7 | −3.5 (2) |
| C14—C13—C9—N1 | −11.8 (2) | C2—C1—C6—C7 | 177.48 (14) |
| C21—C13—C9—N1 | 169.30 (13) | O3—C7—C6—C5 | −33.6 (2) |
| C14—C13—C9—C8 | 110.44 (17) | C8—C7—C6—C5 | −159.93 (15) |
| C21—C13—C9—C8 | −68.46 (18) | O3—C7—C6—C1 | 148.42 (14) |
| C9—N1—C1—C2 | −165.72 (14) | C8—C7—C6—C1 | 22.1 (2) |
| C9—N1—C1—C6 | 15.3 (2) | C7—C8—C10—C11 | 51.00 (19) |
| O1—C16—C17—C18 | 179.88 (14) | C9—C8—C10—C11 | 173.74 (14) |
| C21—C16—C17—C18 | −0.5 (2) | N1—C1—C2—C3 | −178.30 (15) |
| C16—C17—C18—C19 | −2.1 (2) | C6—C1—C2—C3 | 0.7 (2) |
| C16—C17—C18—C22 | 177.53 (16) | C7—O3—C12—C11 | −59.8 (2) |
| C17—C18—C19—C20 | 2.0 (3) | C1—C6—C5—C4 | −0.1 (3) |
| C22—C18—C19—C20 | −177.66 (16) | C7—C6—C5—C4 | −178.11 (18) |
| C18—C19—C20—C21 | 0.8 (3) | C6—C5—C4—C3 | 0.7 (3) |
| C16—C21—C20—C19 | −3.3 (2) | C5—C4—C3—C2 | −0.5 (3) |
| C13—C21—C20—C19 | 177.62 (15) | C1—C2—C3—C4 | −0.2 (3) |
| N1—C9—C8—C7 | 59.54 (15) | O3—C12—C11—C10 | 56.8 (2) |
| C13—C9—C8—C7 | −65.06 (16) | C8—C10—C11—C12 | −52.7 (2) |
| N1—C9—C8—C10 | −63.82 (17) |