| Agilent Xcalibur (Ruby, Gemini) diffractometer | 3012 independent reflections |
| Radiation source: Enhance (Cu) X-ray Source | 2873 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.033 |
| Detector resolution: 10.5081 pixels mm-1 | θmax = 75.9°, θmin = 4.4° |
| ω scans | h = −9→9 |
| Absorption correction: analytical [CrysAlis PRO (Agilent, 2010), based on expressions derived by Clark & Reid (1995)] | k = −11→7 |
| Tmin = 0.049, Tmax = 0.198 | l = −24→25 |
| 5248 measured reflections |
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