Table 2.
Degree of conversion (DC) and polymerization rate (PR) of adhesives with different initiator systems and various amount of PA (n=3).
| Degree of Conversion (DC, %) |
||||
|---|---|---|---|---|
| 0-PA (0/60/40)* |
2.5-PA (1.5/60/38.5) |
5-PA (3/60/37) |
10-PA (6/60/34) |
|
| CQ/A | 64.07 ± 0.64a,A | 62.16 ± 0.30a,b,A | 60.9 ± 0.50b,A | 56.94 ± 1.59c,A |
| CQ/A/I-1 | 69.53 ± 0.35a,B | 66.00 ± 0.66b,B | 63.53 ± 0.43c,B | 59.45 ± 0.52d,A,B |
| CQ/A/I-2 | 68.44 ± 1.06a,B | 69.00 ± 0.27a,C | 67.26 ± 0.35a,C | 61.49 ± 0.84b,B,C |
| TPO | 77.57 ± 0.63a,C | 74.11 ± 0.34b,D | 71.28 ± 0.19c,D | 63.98 ± 0.72d,C |
| Polymerization Rate (PR, %/s) |
||||
| 0-PA (0/60/40) |
2.5-PA (1.5/60/38.5) |
5-PA (3/60/37) |
10-PA (6/60/34) |
|
| CQ/A | 4.92 ± 0.08a,A | 5.19 ± 0.25a,A | 6.49 ± 0.23b,A | 4.98 ± 0.45a,A |
| CQ/A/I-1 | 16.76 ± 0.21a,B | 9.96 ± 0.51b,B | 9.12 ± 0.42b,c,A | 7.86 ± 0.73c,B |
| CQ/A/I-2 | 17.45 ± 0.86a,B | 13.19 ± 0.57b,C | 15.03 ± 2.23a,b,B | 12.35 ± 0.33b,C |
| TPO | 24.43 ± 1.34a,C | 20.29 ± 1.66a,b,D | 19.64 ± 1.58b,c,C | 15.92 ± 1.82c,D |
Ratio in parenthesis indicates the PA/resin/ethanol weight ratio of each formulation.
Values with same lower case letters are statistically equivalent within the same initiator formulation.
Values with same capital letters are statistically equivalent within the same PA concentration.