Table 13.
entry | product | yield(%) | ee(%) |
---|---|---|---|
1 | 46 | 90 | |
2 | 32 | 84 | |
3 | 49 | 93 | |
4 | 74 | 64 | |
5 | 92 | 91 | |
6 | 86 | 77 | |
7 | 98 | 87 | |
8 | 90 | 89 | |
9 | 91 | 70 | |
10 | 56 | 46 | |
11 | 40 | 34 | |
12 | 48 | 20 | |
13 | 97 | 92 | |
14 | 69 | 90 | |
15 | 84 | 62 | |
16 | 92 | 42 | |
17 | 26 | 31 | |
18 | 88 | 9 | |
19 | 9 | 67 | |
20 | 21 | 45 | |
21 | 36 | 31 | |
22 | 88 | 87 |
Ts = p-toluenesulfonyl; Mbs = 4-methoxybenzenesulfonyl; TMS = trimethylsilyl.