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. Author manuscript; available in PMC: 2014 Feb 20.
Published in final edited form as: J Am Chem Soc. 2013 Feb 11;135(7):2478–2481. doi: 10.1021/ja312311k

Table 1.

Convergent assembly of piperidines with terminal acetylene equivalent.a

graphic file with name nihms445091t1.jpg
a

Yields correspond to isolated product after silica gel chromatography and represent overall yields from the imine precursor 6. Diastereoselectivity was determined by 1H NMR of the crude reaction mixture.

b

Conducted using HF-pyridine in THF at 0 °C.