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. 2012 Dec 8;69(Pt 1):o61. doi: 10.1107/S1600536812049847
Bruker APEXII CCD diffractometer 2433 independent reflections
Radiation source: fine-focus sealed tube 1666 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.030
Detector resolution: 0.3 pixels mm-1 θmax = 26.0°, θmin = 1.7°
φ and ω scans h = −16→16
Absorption correction: multi-scan (SADABS; Bruker, 2006) k = −6→7
Tmin = 0.936, Tmax = 0.987 l = −20→20
7373 measured reflections