| Refinement on F2 | Primary atom site location: structure-invariant direct methods |
| Least-squares matrix: full | Hydrogen site location: difference Fourier map |
| R[F2 > 2σ(F2)] = 0.038 | H-atom parameters constrained |
| wR(F2) = 0.100 | Method = Modified Sheldrick w = 1/[σ2(F2) + (0.06P)2 + 1.04P], where P = (max(Fo2,0) + 2Fc2)/3 |
| S = 0.99 | (Δ/σ)max = 0.002 |
| 3891 reflections | Δρmax = 0.26 e Å−3 |
| 271 parameters | Δρmin = −0.25 e Å−3 |
| 0 restraints |