| Bruker Kappa APEXII CCD diffractometer | 6537 independent reflections |
| Radiation source: fine-focus sealed tube | 5993 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.024 |
| φ and ω scans | θmax = 30.0°, θmin = 2.2° |
| Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −10→10 |
| Tmin = 0.89, Tmax = 0.96 | k = −13→13 |
| 29040 measured reflections | l = −22→22 |