| Bruker APEX CCD diffractometer | 2866 independent reflections |
| Radiation source: fine-focus sealed tube | 2551 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.045 |
| Frames, each covering 0.3 ° in ω scans | θmax = 25.0°, θmin = 1.9° |
| Absorption correction: multi-scan (SADABS; Bruker, 2003) | h = −7→7 |
| Tmin = 0.984, Tmax = 0.994 | k = −14→14 |
| 15459 measured reflections | l = −25→25 |
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