Table 3. Positions (cm–1) of Distinctive Bands in the Mid Infrared Spectra of Polymorphs of 1.
polymorph |
|||||
---|---|---|---|---|---|
section | type | 1-I | 1-III | 1–112 | 1–107 |
a | ν(O–H) | 3315 | 3264 | 3379 | 3555 |
b | ν(C=O) | 1683 | 1689 | 1690 | 1682 |
c | ν(C–O) | 1280, 1235 | 1284, 1236 | 1285, 1220 | 1288, 1219 |
d | ν(C–C–O) [in phase] | 957 | 967 | 975 | 958 |
e | ν(C–H) [banding wagging] | 772 | 772 | 775 | 780 |