Table I.
Data Collection and Refinement Statistics
| 4SS-insulin | |
|---|---|
| Data collection | |
| Space group | R 3 |
| Cell dimensions | |
| a, b, c (Å) | 79.37, 79.37, 34.23 |
| α, β, γ (°) | 90.00, 90.00, 120.00 |
| Resolution (Å) | 50–1.98 (2.01–1.98) |
| Rsym | 0.049 (0.202) |
| I/σI | 31.6 (2.7) |
| Completeness (%) | 97.0 (57.4) |
| Redundancy | 5.3 (1.6) |
| Refinement | |
| Resolution (Å) | 39.7–1.98 |
| No. reflections | 5284 |
| Rwork/Rfree | 0.21/0.28 |
| No. atoms | |
| Protein | 762 |
| Ligand/ion | 2 |
| Water | 33 |
| B-factors | |
| Protein | 25.1 |
| Ligand/ion | 25.0 |
| Water | 32.3 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.015 |
| Bond angles (°) | 2.023 |