Table 2. Data collection and refinement statistics.
| Pt-derivative | Native | |
| Data collection | ||
| Space group | P6(5) | P6(5) |
| Cell dimensions | ||
| a, b, c (Å) | 109.13, 109.13, 130.03 | 109.38, 109.38, 129.44 |
| α, β, γ (°) | 90, 90, 120 | 90, 90, 120 |
| Resolution (Å)* | 50-3.10 (3.21-3.10) | 50-2.40 (2.46-2.40) |
| Rsym (%)* | 12.8 (61.4) | 6.0 (61.6) |
| I/σI* | 37.0 (4.3) | 33.2 (3.3) |
| Completeness (%)* | 100 (100) | 100 (100) |
| Redundancy* | 22.5 (21.9) | 11.4 (11.3) |
| Refinement | ||
| Resolution (Å) | 50-2.40 | |
| No. reflections | 32,630 | |
| Rwork/Rfree | 20.9/24.1 | |
| No. atoms | ||
| Protein | 2944 | |
| Ligand/ion | 166 | |
| Water | 218 | |
| B-factors | ||
| Protein | 31.2 | |
| Ligand/ion | 84.1 | |
| Water | 32.8 | |
| RMS deviations | ||
| Bond lengths (Å) | 0.003 | |
| Bond angles (°) | 0.760 |
One crystal was used for each data set.
<?ENTCHAR ast?>: Values in parentheses are for the highest-resolution shell.