Table 1. Data-collection statistics.
Values in parentheses are for the highest-resolution shell.
| No. of crystals | 1 |
| Beamline | A1, Cornell High Energy Synchrotron Source |
| Wavelength | 0.977 |
| Detector | Quantum 210 CCD detector |
| Crystal–detector distance (mm) | 480 |
| Rotation range per image (°) | 1 |
| Total rotation range (°) | 360 |
| Exposure time per image (s) | 60 |
| Resolution range (A) | 50–5.07 (5.16–5.07) |
| Space group† | P212121 |
| Unit-cell parameters (A,°) | a = 143.9, b = 167.6, c = 531.0, α = β = γ = 90 |
| Mosaicity (°) | 0.300 |
| Total no. of reflections | 259264 |
| Unique reflections | 44222 |
| Multiplicity | 3.8 (3.7) |
| 〈I/σ(I)〉 | 14.9 (1.7) |
| Completeness (%) | 83.7 (46.3) |
| R merge ‡ (%) | 0.202 (0.412) |
| Overall B factor from Wilson plot (Å2) | 247.7 |
| Optical resolution | 3.89 |
†
Space-group assignment is based on the low metric tensor distortion index for primitive orthorhombic determined by HKL-2000 and the presence of h = odd, k = odd and l = odd systematic absences in the h00, 0k0 and 00l directions, respectively. We do not yet know the exact number of molecules in the asymmetric unit. Values of 1, 2, 3 and 4 would yield solvent contents of 86.4, 72.8, 59.3 and 45.7%, respectively.
‡
R
merge = 
.