Table 1. Data-collection statistics for β-mannosidase crystals.
Values in parentheses are for the highest-resolution shell.
| Native | I3C derivative | |
|---|---|---|
| Space group | P1 | P1 |
| Unit-cell parameters (Å, °) | a = 62.37, b = 69.73, c = 69.90, α = 108.20, β = 101.51, γ = 103.20 | a = 61.82, b = 65.23, c = 68.72, α = 108.63, β = 101.06, γ = 103.06 |
| Wavelength (Å) | 0.9180 | 1.5419 |
| Resolution (Å) | 40.91–2.41 (2.54–2.41) | 40.28–2.44 (2.58–2.44) |
| R merge † | 0.188 (0.804) | 0.125 (0.605) |
| 〈I/σ(I)〉 | 7.8 (2.2) | 7.4 (2.0) |
| Completeness (%) | 97.7 (91.8) | 90.7 (88.5) |
| Multiplicity | 3.9 (3.8) | 3.9 (3.8) |
| No. of reflections | 154978 (20449) | 124224 (17536) |
| No. of unique reflections | 39352 (5358) | 31919 (4545) |
| Matthews coefficient (Å3 Da−1) | 2.56 | 2.34 |
| Molecules in assymetric unit | 1 | 1 |
R
merge =
.