Table 2.
13C NMR Data for Compounds 1-3 (125 MHz, CDCl3)
| carbon | 1 | 2 | 3 |
|---|---|---|---|
| 1 | 108.3 | 108.5 | 108.4 |
| 1a | 18.1 | 17.9 | 18.1 |
| 2 | 157.2 | 157.5 | 157.1 |
| 3 | 109.2 | 114.2 | 109.1 |
| 4 | 162.9 | 162.8 | 163.0 |
| 5 | 110.0 | 109.2 | 110.2 |
| 6 | 159.8 | 159.6 | 159.9 |
| 7 | 205.4 | 205.4 | 205.6 |
| 8 | 33.8 | 33.8 | 34.1 |
| 9 | 8.9 | 22.9 | 9.2 |
| 1′ | 108.5 | 108.5 | 108.4 |
| 2′ | 157.7 | 157.5 | 157.1 |
| 3′ | 114.2 | 114.2 | 109.1 |
| 4′ | 162.9 | 162.8 | 163.0 |
| 5′ | 109.2 | 109.2 | 110.2 |
| 6′ | 159.6 | 159.6 | 159.9 |
| 7′ | 205.4 | 205.4 | 205.6 |
| 8′ | 33.8 | 33.8 | 34.1 |
| 9′ | 22.9 | 22.9 | 9.2 |
| OCH3 | 62.1 63.0 |
63.0 63.0 |
62.2 62.2 |
| 1″ | 122.7 | 122.7 | |
| 2″ | 132.2 | 132.2 | |
| 3″ | 18.0 | 17.9 | |
| 4″ | 25.8 | 25.8 | |
| 1″′ | 122.7 | ||
| 2″′ | 132.2 | ||
| 3″′ | 17.9 | ||
| 4″′ | 25.8 |