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. Author manuscript; available in PMC: 2013 Sep 21.
Published in final edited form as: J Chromatogr A. 2012 Jul 25;1256:89–97. doi: 10.1016/j.chroma.2012.07.052

Table 3.

Precision and accuracy for Method 1 and Method 2.

Intra-assay
0.1 uM 0.25 uM
Avg (μM) Bias (%) RSD (%) Avg (μM) Bias (%) RSD (%) Avg (μM)
T1AM 0.11 9 13 40.6
T0AM 0.10 −2 13 39.3
Ac-T1AM 0.10 −3 15 44.3
S-T1AM 0.22 −12 7 41.7
TA1 0.24 −4 13 38.4
TA0 0.24 −2 13 40.2
Inter-assay
0.1 uM 0.25 uM
Avg (μM) Bias (%) RSD (%) Avg (μM) Bias (%) RSD (%) Avg (μM)
T1AM 0.10 2 19 40.8
T0AM 0.11 9 17 41.3
Ac-T1AM 0.12 15 12 42.5
S-T1AM 0.22 −12 16 38.9
TA1 0.26 4 10 39.9
TA0 0.26 3 11 42.1

n = 4–7 per analyte