Table 3.
Retention time (min) | Mass (m/z) | Non-DP | DP | P |
---|---|---|---|---|
ES (+) mode | ||||
20.04 | 1461.2680 | 6.61 ± 1.43 | 7.38 ± 2.09 | 0.009 |
17.18 | 1039.724 | 153.13 ± 44.87 | 134.44 ± 52.43 | 0.010 |
17.15 | 520.3663 | 304.62 ± 48.29 | 282.22 ± 53.29 | 0.015 |
20.27 | 1494.291 | 18.50 ± 4.16 | 20.03 ± 4.99 | 0.022 |
17.3 | 502.3353 | 15.82 ± 5.11 | 14.21 ± 4.05 | 0.024 |
17.46 | 546.3991 | 41.14 ± 17.33 | 35.35 ± 14.02 | 0.034 |
19.71 | 1376.208 | 20.36 ± 6.07 | 23.05 ± 8.81 | 0.037 |
18.35 | 269.2497 | 4.13 ± 1.26 | 3.66 ± 1.15 | 0.042 |
17.69 | 1043.763 | 113.36 ± 46.83 | 96.79 ± 36.09 | 0.044 |
21.13 | 237.1001 | 26.71 ± 11.22 | 30.31 ± 10.32 | 0.046 |
17.68 | 1565.1790 | 4.15 ± 2.49 | 3.33 ± 1.53 | 0.047 |
29.01 | 195.0539 | 5.93 ± 1.88 | 6.57 ± 1.97 | 0.048 |
ES (−) mode | ||||
17.14 | 1019.5881 | 10.58 ± 5.27 | 8.77 ± 5.09 | 0.010 |
0.6 | 444.6674 | 1.32 ± 0.95 | 1.55 ± 0.82 | 0.013 |
0.53 | 740.8311 | 5.84 ± 2.06 | 6.63 ± 2.25 | 0.015 |
17.5 | 590.3351 | 104.35 ± 42.97 | 88.28 ± 38.06 | 0.017 |
29.23 | 599.3050 | 2.50 ± 0.82 | 2.20 ± 0.69 | 0.015 |
29.23 | 288.1364 | 3.15 ± 1.06 | 3.47 ± 1.01 | 0.029 |
0.53 | 462.8737 | 1.23 ± 0.49 | 1.44 ± 0.59 | 0.032 |
17.53 | 658.3196 | 4.30 ± 1.33 | 3.89 ± 0.98 | 0.038 |
19.87 | 961.5879 | 7.01 ± 3.20 | 8.21 ± 3.71 | 0.042 |
Data are presented as mean normalized peak areas ± SD. The P value was calculated by Mann-Whitney U test.