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. 2011 Jun;7(2):137–144.

Table 4.

Evaluation of the accuracy and precision data of the proposed method for the determination of NF nd TZ in Conaz tablet

Norfloxacin
Amount added (μg/mL) 6.00
8.00
10.00
Amount found (μg/mL) % Found Amount found (μg/mL) % Found Amount found (μg/mL) % Found

  Intra-day 6.01 100.21 8.04 100.50 10.00 100.00
6.00 100.00 8.01 100.13 9.92 99.20
6.03 100.51 8.06 100.75 10.08 100.80
  % R ± SD 100.24 ± 0.26 100.46 ± 0.31 100 ± 0.80
  % RSD 0.26 0.31 0.80
  % Er 0.15 0.18 0.46
  Inter-day 6.03 100.51 8.01 100.13 10.00 100.00
6.04 100.66 7.94 99.27 9.95 99.50
5.98 99.67 7.96 99.50 10.03 100.30
  % R ± SD 100.28 ± 0.53 99.63 ± 0.45 99.93 ± 0.40
  % RSD 0.53 0.45 0.40
  % Er 0.31 0.26 0.23
Tinidazole
Amount added (μg/mL) 9.00 12.00 15.00

  Intra-day 8.99 99.89 11.95 99.58 15.05 100.33
8.97 99.68 11.91 99.23 15.07 100.47
8.93 99.22 11.97 99.79 14.96 99.73
  % R ± SD 99.60 ± 0.34 99.53 ± 0.28 100.18 ± 0.39
  % RSD 0.34 0.28 0.39
  % Er 0.20 0.16 0.23
  Inter-day 8.99 99.89 11.97 99.79 15.05 100.33
8.95 99.43 12.02 100.16 15.02 100.13
9.02 100.17 12.04 100.35 14.98 99.87
  % R ± SD 99.83 ± 0.37 100.1 ± 0.28 100.11 ± 0.23
  % RSD 0.37 0.28 0.23
  % Er 0.21 0.16 0.13

Each result is the mean recovery of three separate determinations. Three samples of NF and TZ were repeated. Batch No. 916 9019.