Table 4.
Evaluation of the accuracy and precision data of the proposed method for the determination of NF nd TZ in Conaz tablet
| Norfloxacin | |||||||||
|---|---|---|---|---|---|---|---|---|---|
| Amount added (μg/mL) | 6.00 |
8.00 |
10.00 |
||||||
| Amount found (μg/mL) | % Found | Amount found (μg/mL) | % Found | Amount found (μg/mL) | % Found | ||||
| Intra-day | 6.01 | 100.21 | 8.04 | 100.50 | 10.00 | 100.00 | |||
| 6.00 | 100.00 | 8.01 | 100.13 | 9.92 | 99.20 | ||||
| 6.03 | 100.51 | 8.06 | 100.75 | 10.08 | 100.80 | ||||
| % R ± SD | 100.24 ± 0.26 | 100.46 ± 0.31 | 100 ± 0.80 | ||||||
| % RSD | 0.26 | 0.31 | 0.80 | ||||||
| % Er | 0.15 | 0.18 | 0.46 | ||||||
| Inter-day | 6.03 | 100.51 | 8.01 | 100.13 | 10.00 | 100.00 | |||
| 6.04 | 100.66 | 7.94 | 99.27 | 9.95 | 99.50 | ||||
| 5.98 | 99.67 | 7.96 | 99.50 | 10.03 | 100.30 | ||||
| % R ± SD | 100.28 ± 0.53 | 99.63 ± 0.45 | 99.93 ± 0.40 | ||||||
| % RSD | 0.53 | 0.45 | 0.40 | ||||||
| % Er | 0.31 | 0.26 | 0.23 | ||||||
| Tinidazole | |||||||||
| Amount added (μg/mL) | 9.00 | 12.00 | 15.00 | ||||||
| Intra-day | 8.99 | 99.89 | 11.95 | 99.58 | 15.05 | 100.33 | |||
| 8.97 | 99.68 | 11.91 | 99.23 | 15.07 | 100.47 | ||||
| 8.93 | 99.22 | 11.97 | 99.79 | 14.96 | 99.73 | ||||
| % R ± SD | 99.60 ± 0.34 | 99.53 ± 0.28 | 100.18 ± 0.39 | ||||||
| % RSD | 0.34 | 0.28 | 0.39 | ||||||
| % Er | 0.20 | 0.16 | 0.23 | ||||||
| Inter-day | 8.99 | 99.89 | 11.97 | 99.79 | 15.05 | 100.33 | |||
| 8.95 | 99.43 | 12.02 | 100.16 | 15.02 | 100.13 | ||||
| 9.02 | 100.17 | 12.04 | 100.35 | 14.98 | 99.87 | ||||
| % R ± SD | 99.83 ± 0.37 | 100.1 ± 0.28 | 100.11 ± 0.23 | ||||||
| % RSD | 0.37 | 0.28 | 0.23 | ||||||
| % Er | 0.21 | 0.16 | 0.13 | ||||||
Each result is the mean recovery of three separate determinations. Three samples of NF and TZ were repeated. Batch No. 916 9019.